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Queen’s Chemistry TA MANUAL Chemistry 112 Name: Department of Chemistry Queen’s University Kingston, Ontario 2013-2014 Edition Table of Contents Laboratory Schedule for 2013/2014. 3 General Notes. 5 Safety Quiz. 7 Experiment 1. Molar Mass of a Volatile Organic Liquid. 9 Experiment 2.
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Gravimetric Analysis. 13 Experiment 3. Spectroscopic Analysis. 15 Experiment 4. Synthesis of Metal Acetyl-acetonate Complex – Part 1. 17 Experiment 5. Recrystallization of Metal Acetyl-acetonate Complex – Part 2.
19 Experiment 6. Polymerization of Polystyrene as an Introduction to Green Chemistry. 21 Experiment 7. Photochemical Reaction with Ferrioxalate.
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25 Experiment 8. Vapour Pressure and Heat of Vaporization. 27 Experiment 9.
Calorimetry – Part 1. 29 Experiment 10. Calorimetry – Part 2. 31 Experiment 11. Gas Laws.
33 Experiment 12. Titration of Vitamin C in Orange Juice and Tang. 37 Experiment 13. Corrosion of Metals. 39 Experiment 14. Qualitative Analysis. 43 Experiment 15.
Titrimetric Analysis. 45 Experiment 16. Diprotic Acid Titration. 47 Experiment 17. Buffer Titration. 51 Experiment 18.
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Rate and Order of a Chemical Reaction. 53 Experiment 19.
Rate Law Determination of the Crystal Violet Reaction. 55 Experiment 20. Synthesis of Aspirin – Part 1. 57 Experiment 21.
Recrystallization and Analysis of Aspirin – Part 2. 59 List of Lab Equipment Errors. 61 Laboratory Schedule for 2013/2014 Fall Term Week 1 Date Sep 9–13 2 Sep 16–20 Lab Lab Safety Training Page All students must attend the lab Experiment 1: Molar Mass of a Volatile Organic Liquid 9 Lab room is CHE 206b; tutorial room is CHE202 or CHE211.
Chemistry 230 Laboratory Manual Chemistry 230 Laboratory Manual CSU Dominguez Hills by Ulrich de la Camp and Oliver Seely All materials directly linked to this Web page, accompanying photos and videos are in the public domain and may be copied without restriction. The following main topics are covered below: Introduction, Required Materials, Direction for Laboratory Work, Appendices and Demonstrations. Although the demonstrations have links within the text of individual exercises, they are offered here separately for easy access. Required Materials Laboratory Points Laboratory Safety The Laboratory Notebook Directions for Laboratory Work Appendices Demonstrations.